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    1-Hydroxy-1

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      1-Hydroxy-1,2-benziodoxol-3-one 1-oxide pyridinium complex

      SKU
      H0104

      Category: Building Blocks, Intermediates, Reagents

      Synonyms
      IBX pyridine complex , PIBX , Pyridinium o-iodoxybenzoate
      1380548-11-7
      CAS-Number
      C12H10INO4
      Molecular Formula
      359.1
      Molecular Weight

      • Product Data
      • Handling
      • Safety Information
      • Details

      Specifications

      Purity
      ≥97% (NMR)
      Identity
      1H-NMR
      Appearance
      White to off-white solid

      Properties

      Solvents
      Soluble in toluene.
      Handling Advice
      Protect from light and moisture.
      Use / Stability
      Stable for at least 2 years after receipt when stored at -20°C.
      Long Term Storage
      -20°C
      Short Term Storage
      +4°C
      Shipping
      AMBIENT
      Transportation
      Not dangerous goods
      Signal word
      Warning
      GHS Symbol
      GHS07
      Precautionary statements
      P261-P280-P305 + P351 + P338
      Hazard statements
      H302 + H312 + H332-H315-H319-H335
      Description
      Stable pyridinium salt of o-iodoxybenzoic acid (PIBX) is a convenient substitute of o-iodoxybenzoic acid (IBX) as an oxidant. PIBX is safer, has neutral properties behaves as an equivalent to IBX in the oxidation of alcohols to ketones or aldehydes in polar solvents and provides higher oxidation rate in THF due to better solubility.
      InChi
      InChI=1S/C7H5IO4.C5H5N/c9-7-5-3-1-2-4-6(5)8(10,11)12-7
      References
      (1) I.M. Kumanyaev, et al.: Mendeleev Commun. 22, 129 (2012)
      InChi Key
      JKZNBOGIALICGN-UHFFFAOYSA-N
      Smiles
      C1=CC=[NH+]C=C1.[O-][I]1(=O)OC(=O)C2=CC=CC=C12

      Stable pyridinium salt of o-iodoxybenzoic acid (PIBX) is a convenient substitute of o-iodoxybenzoic acid (IBX) as an oxidant. PIBX is safer, has neutral properties behaves as an equivalent to IBX in the oxidation of alcohols to ketones or aldehydes in polar solvents and provides higher oxidation rate in THF due to better solubility.

      SKU: H0104 Category: Building Blocks, Intermediates, Reagents
      • Additional information

      Additional information

      Synonyms

      IBX pyridine complex, PIBX, Pyridinium o-iodoxybenzoate

      Purity

      ≥97% (NMR)

      Appearance

      White to off-white solid

      CAS-Number

      1380548-11-7

      Molecular Formula

      C12H10INO4

      Molecular Weight

      359.1

      Identity

      1H-NMR

      Solvents

      Soluble in toluene.

      Smiles

      C1=CC=[NH+]C=C1.[O-][I]1(=O)OC(=O)C2=CC=CC=C12

      InChi Key

      JKZNBOGIALICGN-UHFFFAOYSA-N

      Shipping

      AMBIENT

      Short Term Storage

      +4°C

      Long Term Storage

      -20°C

      Handling Advice

      Protect from light and moisture.

      Use / Stability

      Stable for at least 2 years after receipt when stored at -20°C.

      Hazard statements

      H302 + H312 + H332-H315-H319-H335

      Precautionary statements

      P261-P280-P305 + P351 + P338

      GHS Symbol

      GHS07

      Signal word

      Warning

      Transportation

      Not dangerous goods

      References

      (1) I.M. Kumanyaev, et al.: Mendeleev Commun. 22, 129 (2012)

      InChi

      InChI=1S/C7H5IO4.C5H5N/c9-7-5-3-1-2-4-6(5)8(10,11)12-7

      Quantity

      1 g, 5 g, Bulk

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